Crystal Structure of Crystal structure of [μ-13,27-ditertbutyl-3,6,9,17,20,23-hexaazatricyclo [23,3,1,111,15]triaconta-1(28),11,13,15 (30),25,26-hexaene-29,30-diolato[κ5N3,N6,N9,O29,O30 :κ5N17,N20,N23,O29,O30]bis(thiocyanato-κN)nickel(II)
Id | 8102541 |
Common name | Crystal structure of [μ-13,27-ditertbutyl-3,6,9,17,20,23-hexaazatricyclo [23,3,1,111,15]triaconta-1(28),11,13,15 (30),25,26-hexaene-29,30-diolato[κ5N3,N6,N9,O29,O30 :κ5N17,N20,N23,O29,O30]bis(thiocyanato-κN)nickel(II) |
Chemical name | Crystal structure of [μ-13,27-ditertbutyl-3,6,9,17,20,23-hexaazatricyclo [23,3,1,111,15]triaconta-1(28),11,13,15 (30),25,26-hexaene-29,30-diolato[κ5N3,N6,N9,O29,O30 :κ5N17,N20,N23,O29,O30]bis(thiocyanato-κN)nickel(II) |
a (Å) | 8.5140(10) |
b (Å) | 10.4120(11) |
c (Å) | 12.5710(14) |
α (°) | 77.422(9) |
β (°) | 79.470(9) |
γ (°) | 81.725(9) |
V (Å3) | 1063.0(2) |
Space group | P -1 |
Temperature (K) | 293(2) |
Rint | 0.0516 |
Publication: Zeitschrift für Kristallographie - New Crystal Structures (2009) 224, 4 693