Crystal Structure of (dl-5,7,7,12,14,14-Hexamethyl-1,4,8,11-tetra- azacyclotetradecane N,N',N'',N''' )-(9,10-dioxophenanthrene-O,O')- cobalt(ii) hexafluorophosphate dichloromethane solvate

Id7102515
Common name(dl-5,7,7,12,14,14-Hexamethyl-1,4,8,11-tetra- azacyclotetradecane N,N',N'',N''' )-(9,10-dioxophenanthrene-O,O')- cobalt(ii) hexafluorophosphate dichloromethane solvate
Chemical name(dl-5,7,7,12,14,14-Hexamethyl-1,4,8,11-tetra-azacyclotetradecane N,N',N'',N''' )-(9,10-dioxophenanthrene-O,O')-cobalt(ii) hexafluorophosphate dichloromethane solvate
a (Å)20.303(4)
b (Å)12.647(2)
c (Å)29.649(10)
α (°)90.00
β (°)101.41(2)
γ (°)90.00
V (Å3)7463(3)
Space groupC 1 2/c 1
Temperature (K)293(2)
Rint0.0785
Publication: Chemical communications (Cambridge, England) (2004) 6 652-653