Crystal Structure of PROBLEM: _diffrn_measured_fraction_theta_full Low ....... 0.938 NoteRESPONSE: This was a difficult crystal, data collection took about two daysto collect. It was twinned, integration parameters had to beadjusted to avoid excessive numbers of rejected reflections as peakshapes were not too good but even then enough bad reflections were rejectedso that the coverage is not > 0.95.
| Id | 7046608 |
| Chemical name | PROBLEM: _diffrn_measured_fraction_theta_full Low ....... 0.938 NoteRESPONSE: This was a difficult crystal, data collection took about two daysto collect. It was twinned, integration parameters had to beadjusted to avoid excessive numbers of rejected reflections as peakshapes were not too good but even then enough bad reflections were rejectedso that the coverage is not > 0.95. |
| a (Å) | 6.2469(5) |
| b (Å) | 11.8129(8) |
| c (Å) | 15.2220(12) |
| α (°) | 69.327(4) |
| β (°) | 88.425(4) |
| γ (°) | 85.373(4) |
| V (Å3) | 1047.54(14) |
| Space group | P -1 |
| Temperature (K) | 100(2) |
| Rint | 0.0434 |
Publication: Dalton transactions (Cambridge, England : 2003) (2018) 47, 27 9114-9127