Crystal Structure of \ 5-Iodo-2,4,6,8,9,10-hexakis(tri-tert-butylsilyl)heptacyclo-\ [4.4.0.0^1,3^.0^2,5^.0^3,9^.0^4,7^.0^8,10^]decagerman-7-ylium\ tetrakis(2,3,5,6-tetrafluorophenyl)borate
Id | 4114972 |
Chemical name | \ 5-Iodo-2,4,6,8,9,10-hexakis(tri-tert-butylsilyl)heptacyclo-\ [4.4.0.0^1,3^.0^2,5^.0^3,9^.0^4,7^.0^8,10^]decagerman-7-ylium\ tetrakis(2,3,5,6-tetrafluorophenyl)borate |
a (Å) | 15.6610(12) |
b (Å) | 17.3370(12) |
c (Å) | 23.302(2) |
α (°) | 87.001(5) |
β (°) | 87.703(4) |
γ (°) | 83.786(4) |
V (Å3) | 6277.3(8) |
Space group | P -1 |
Temperature (K) | 120 |
Rint | 0.0839 |
Publication: Journal of the American Chemical Society (2002) 124, 8776-8777