Crystal Structure of Dicarbonyl-3κ^2^<i>C</i>-(μ~3~-3,6-dimethyl- 3,6-diazaoctane-1,8-dithiolato- 1:2:3κ^7^<i>S</i>:<i>S</i>,<i>N</i>,<i>N</i>,<i>S</i>':<i>S</i>, <i>S</i>')(μ~2~-3,6-dimethyl-3,6-diazaoctane-1,8-dithiolato- 1:2κ^5^<i>S</i>,<i>N</i>,<i>N</i>',<i>S</i>':<i>S</i>)-1,2-diiron(II)- 3-nickel(0)
Id | 2230442 |
Chemical name | dicarbonyl-3κ^2^<i>C</i>-(μ~3~-3,6-dimethyl- 3,6-diazaoctane-1,8-dithiolato- 1:2:3κ^7^<i>S</i>:<i>S</i>,<i>N</i>,<i>N</i>,<i>S</i>':<i>S</i>, <i>S</i>')(μ~2~-3,6-dimethyl-3,6-diazaoctane-1,8-dithiolato- 1:2κ^5^<i>S</i>,<i>N</i>,<i>N</i>',<i>S</i>':<i>S</i>)-1,2-diiron(II)- 3-nickel(0) |
a (Å) | 8.4051(3) |
b (Å) | 12.7146(5) |
c (Å) | 13.3451(5) |
α (°) | 70.4750(10) |
β (°) | 83.2080(10) |
γ (°) | 79.3090(10) |
V (Å3) | 1318.38(9) |
Space group | P -1 |
Temperature (K) | 173(2) |
Rint | 0.0220 |
Publication: Acta Crystallographica Section E (2011) 67, 6 m766-m767