Crystal Structure of Μ-Acetato-κ^2^<i>O</i>:<i>O</i>-[7,23-dibenzyl-15,31-dichloro- 3,7,11,19,23,27-hexaazatricyclo[27.3.1.1^13,17^]tetratriconta- 1(32),2,11,13,15,17(34),18,27,29(33),30- decaene-33,34-diolato-κ^10^<i>N</i>^4^,<i>N</i>^5^,<i>N</i>^6^,<i>O</i>^1^, <i>O</i>^2^:<i>N</i>^1^,<i>N</i>^2^,<i>N</i>^3^,<i>O</i>^1^,<i>O</i>^2^] dinickel perchlorate acetonitrile disolvate
Id | 2217097 |
Chemical name | μ-Acetato-κ^2^<i>O</i>:<i>O</i>-[7,23-dibenzyl-15,31-dichloro- 3,7,11,19,23,27-hexaazatricyclo[27.3.1.1^13,17^]tetratriconta- 1(32),2,11,13,15,17(34),18,27,29(33),30- decaene-33,34-diolato-κ^10^<i>N</i>^4^,<i>N</i>^5^,<i>N</i>^6^,<i>O</i>^1^, <i>O</i>^2^:<i>N</i>^1^,<i>N</i>^2^,<i>N</i>^3^,<i>O</i>^1^,<i>O</i>^2^] dinickel perchlorate acetonitrile disolvate |
a (Å) | 16.7957(14) |
b (Å) | 17.2146(15) |
c (Å) | 18.0209(15) |
α (°) | 90.00 |
β (°) | 99.305(2) |
γ (°) | 90.00 |
V (Å3) | 5141.8(8) |
Space group | P 1 21/n 1 |
Temperature (K) | 273(2) |
Rint | 0.0605 |
Publication: Acta Crystallographica Section E (2008) 64, 1 m18-m18