Crystal Structure of [13,27-Dimethyl-3,6,9,17,20,23-hexaazatricyclo[23.3.1.1^11,15^]triaconta- 1(29),2,9,11,13,15(30),16,23,25,27-decaene-29,30-diol- κ^5^N^3^,N^6^,N^9^,O^29^,O^30^]bis(nitrato-κ^2^O,O)lutetium(III)—– nitrate—–water—–ethyl acetate (1/1/0.5/0.25)

Id2213818
Chemical name[13,27-Dimethyl-3,6,9,17,20,23-hexaazatricyclo[23.3.1.1^11,15^]triaconta- 1(29),2,9,11,13,15(30),16,23,25,27-decaene-29,30-diol- κ^5^N^3^,N^6^,N^9^,O^29^,O^30^]bis(nitrato-κ^2^O,O)lutetium(III)—– nitrate—–water—–ethyl acetate (1/1/0.5/0.25)
a (Å)24.649(3)
b (Å)14.0182(11)
c (Å)21.4453(17)
α (°)90.00
β (°)102.307(2)
γ (°)90.00
V (Å3)7239.8(12)
Space groupC 1 c 1
Temperature (K)291(2)
Rint0.0503
Publication: Acta Crystallographica Section E (2007) 63, 6 m1668-m1669