Crystal Structure of Acetato[μ-10,21-dibutyl-3,6,14,17-tetrazatricyclo[17.3.1.1^(8,12)^]tetracosa- 1(23),2,6,8,10,12(24),13,17,19,21-decaene-23,24-diolato(2-)- κ^4^N^3^,N^6^,O^23^,O^24^:κ^4^N^14^,N^17^,O^23^,O^24^]dinickel(II) perchlorate acetonitrile hemisolvate
Id | 2210842 |
Chemical name | Acetato[μ-10,21-dibutyl-3,6,14,17-tetrazatricyclo[17.3.1.1^(8,12)^]tetracosa- 1(23),2,6,8,10,12(24),13,17,19,21-decaene-23,24-diolato(2-)- κ^4^N^3^,N^6^,O^23^,O^24^:κ^4^N^14^,N^17^,O^23^,O^24^]dinickel(II) perchlorate acetonitrile hemisolvate |
a (Å) | 31.353(2) |
b (Å) | 11.2316(7) |
c (Å) | 21.2808(14) |
α (°) | 90.00 |
β (°) | 116.8750(10) |
γ (°) | 90.00 |
V (Å3) | 6684.5(7) |
Space group | C 1 2/c 1 |
Temperature (K) | 298(2) |
Rint | 0.045 |
Publication: Acta Crystallographica Section E (2006) 62, 10 m2442-m2444