Crystal Structure of Acetato[μ-10,21-dibutyl-3,6,14,17-tetrazatricyclo[17.3.1.1^(8,12)^]tetracosa- 1(23),2,6,8,10,12(24),13,17,19,21-decaene-23,24-diolato(2-)- κ^4^N^3^,N^6^,O^23^,O^24^:κ^4^N^14^,N^17^,O^23^,O^24^]dinickel(II) perchlorate acetonitrile hemisolvate

Id2210842
Chemical nameAcetato[μ-10,21-dibutyl-3,6,14,17-tetrazatricyclo[17.3.1.1^(8,12)^]tetracosa- 1(23),2,6,8,10,12(24),13,17,19,21-decaene-23,24-diolato(2-)- κ^4^N^3^,N^6^,O^23^,O^24^:κ^4^N^14^,N^17^,O^23^,O^24^]dinickel(II) perchlorate acetonitrile hemisolvate
a (Å)31.353(2)
b (Å)11.2316(7)
c (Å)21.2808(14)
α (°)90.00
β (°)116.8750(10)
γ (°)90.00
V (Å3)6684.5(7)
Space groupC 1 2/c 1
Temperature (K)298(2)
Rint0.045
Publication: Acta Crystallographica Section E (2006) 62, 10 m2442-m2444