Crystal Structure of Di-μ-cyano-1:2κ^2^C:N;1:3κ^2^C:N-tetracyano-1κ^4^N-bis(13-ethyl-5,7,7- trimethyl-13-nitro-1,4,8,11-tetraazacyclotetradec-4-ene)- 2κ^4^N^1^,N^4^,N^8^,N^11^;3κ^4^N^1^,N^4^,N^8^,N^11^-dicopper(II)nickel(II) diaqua-1,3κ^2^O-di-μ-cyano-1:2κ^2^C:N;1:3κ^2^C:N-tetracyano-1κ^4^N- bis(13-ethyl-5,7,7-trimethyl-13-nitro-1,4,8,11-tetraazacyclotetradec-4-ene)- 2κ^4^N^1^,N^4^,N^8^,N^11^;3κ^4^N^1^,N^4^,N^8^,N^11^-dicopper(II)nickel(II) bis[tetracyanonickelate(II)] octahydrate
| Id | 2014211 |
| Chemical name | di-μ-cyano-1:2κ^2^C:N;1:3κ^2^C:N-tetracyano-1κ^4^N-bis(13-ethyl-5,7,7- trimethyl-13-nitro-1,4,8,11-tetraazacyclotetradec-4-ene)- 2κ^4^N^1^,N^4^,N^8^,N^11^;3κ^4^N^1^,N^4^,N^8^,N^11^-dicopper(II)nickel(II) diaqua-1,3κ^2^O-di-μ-cyano-1:2κ^2^C:N;1:3κ^2^C:N-tetracyano-1κ^4^N- bis(13-ethyl-5,7,7-trimethyl-13-nitro-1,4,8,11-tetraazacyclotetradec-4-ene)- 2κ^4^N^1^,N^4^,N^8^,N^11^;3κ^4^N^1^,N^4^,N^8^,N^11^-dicopper(II)nickel(II) bis[tetracyanonickelate(II)] octahydrate |
| a (Å) | 11.7497(2) |
| b (Å) | 14.0540(3) |
| c (Å) | 17.9014(4) |
| α (°) | 70.1540(10) |
| β (°) | 78.1650(10) |
| γ (°) | 81.2900(10) |
| V (Å3) | 2710.63(10) |
| Space group | P -1 |
| Temperature (K) | 120(2) |
| Rint | 0.0628 |
Publication: Acta Crystallographica Section C (2004) 60, 8 m410-m413